Journal article
Improved 29Si NMR detection of sterically protected fluorosilanes using the 29Si(19F)-INEPT technique.



Publication Details
Authors:
Pietschnig, R.
Publisher:
Elsevier B.V.DO - 10.1016/j.jfluchem.2006.10.012
Publication year:
2007
Journal:
Journal of Fluorine Chemistry
Pages range:
150-152
Volume number:
128
Start page:
150
End page:
152
ISSN:
0022-1139

Abstract
The 29Si-19F INEPT NMR method was applied to significantly reduce the recording time of 29Si NMR spectra of sterically shielded fluorosilanes. This technique also improves the signal to noise ratio to a degree which allows the simultaneous detection of minor byproducts which are below the detection limit using direct acquisition. [on SciFinder(R)]


Keywords
fluorosilane detection Si29 F19 NMR INEPT technique


Authors/Editors

Last updated on 2019-25-07 at 16:00