Journal article
Determination of the strain-rate sensitivity of ultrafine-grained materials by spherical nanoindentation
Publication Details
Authors: | Feldner, P.; Merle, B.; Göken, M. |
Publisher: | CAMBRIDGE UNIV PRESS |
Publication year: | 2017 |
Journal: | Journal of Materials Research |
Pages range : | 1466-1473 |
Volume number: | 32 |
Issue number: | 8 |
Start page: | 1466 |
End page: | 1473 |
Number of pages: | 8 |
ISSN: | 0884-2914 |
DOI-Link der Erstveröffentlichung: |
Abstract
The strain-rate sensitivity of the flow stress represents a crucial parameter for characterizing the deformation kinetics of a material. In this work a new method was developed and validated for determining the local strain-rate sensitivity of the flow stress at different plastic strains. The approach is based on spherical nanoindentation strain-rate jump tests during one deformation experiment. In the case of ultrafine-grained Al and ultrafine-grained Cu good agreement between this technique and macroscopic compression tests has been achieved. In contrast to this, individual spherical nanoindentation experiments at constant strain-rates resulted in unrealistically high strain-rate sensitivities for both materials because of drift influences. Microstructural investigations of the residual spherical imprints on ultrafine-grained Al and ultrafine-grained Cu revealed significant differences regarding the deformation structure. For ultrafine-grained Cu considerably less activity of grain boundary sliding has been observed compared to ultrafinegrained Al.
The strain-rate sensitivity of the flow stress represents a crucial parameter for characterizing the deformation kinetics of a material. In this work a new method was developed and validated for determining the local strain-rate sensitivity of the flow stress at different plastic strains. The approach is based on spherical nanoindentation strain-rate jump tests during one deformation experiment. In the case of ultrafine-grained Al and ultrafine-grained Cu good agreement between this technique and macroscopic compression tests has been achieved. In contrast to this, individual spherical nanoindentation experiments at constant strain-rates resulted in unrealistically high strain-rate sensitivities for both materials because of drift influences. Microstructural investigations of the residual spherical imprints on ultrafine-grained Al and ultrafine-grained Cu revealed significant differences regarding the deformation structure. For ultrafine-grained Cu considerably less activity of grain boundary sliding has been observed compared to ultrafinegrained Al.